Valorization of Mango Peels for Pectin Production: Process Optimization and Physicochemical Evaluation

Authors

DOI:

https://doi.org/10.29105/idcyta.v11i2.167

Keywords:

Pectin, Green Chemistry, Degree of Esterification, Water Holding Capacity, Oil Holding Capacity

Abstract

Agro-industrial residues constitute a sustainable, low-cost resource for obtaining bioactive compounds, while also representing an environmental problem. In this context, extracting pectin from mango peels would contribute to establishing a circular economy in the agro-industrial sector, as it would mitigate disposal issues by valorizing these by-products. Pectin was obtained from mango peels by extraction with a 0.1 M citric acid solution at a solid-to-liquid ratio of 1:20. To identify the effect of temperature (60, 75, and 90°C) and time (30, 60, and 90 min) on the yield, a 3² factorial design was used. It was found that high-methoxyl pectin was obtained in all treatments; according to the regression model, the optimal extraction conditions were 75°C and 90 min, with which a yield of 26.34% was obtained. Under these conditions, the degree of esterification (DE) of the extracted pectin was 92.37%, and the water retention capacity (WRC) and oil retention capacity (ORC) were 1.12± 0.04 g/g and 2.07 ± 0.16 g/g, respectively. The extracted pectin has potential to be a thickening, gelling, and stabilizing agent.

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References

Chen, J., Cheng, H., Zhi, Z., Zhang, H., Linhardt, R. J., Zhang, F., Chen, S., & Ye, X. (2021). Extraction temperature is a decisive factor for the properties of pectin. Food Hydrocolloids, 112, 106160. https://doi.org/10.1016/j.foodhyd.2020.106160 DOI: https://doi.org/10.1016/j.foodhyd.2020.106160

Dixit, S. S., Muruganandam, L., & Ganesh Moorthy, I. (2025). Pectin from fruit peel: A comprehensive review on various extraction approaches and their potential applications in pharmaceutical and food industries. Carbohydrate Polymer Technologies and Applications, 9, 100708. https://doi.org/10.1016/j.carpta.2025.100708 DOI: https://doi.org/10.1016/j.carpta.2025.100708

Durán, R., Villa, A. L., Ribeiro, R., & Rabi, J. A. (2015). Pectin extraction from mango peels in batch reactor: Dynamic one-dimensional modeling and lattice Boltzmann simulation. Chemical Product and Process Modeling, 10(3), 203–210. https://doi.org/10.1515/cppm-2015-0014 DOI: https://doi.org/10.1515/cppm-2015-0014

El Fihry, N., El Mabrouk, K., Eeckhout, M., Schols, H. A., & Hajjaj, H. (2024). Physicochemical, structural, and functional characterization of pectin extracted from quince and pomegranate peel: A comparative study. International Journal of Biological Macromolecules, 256, 127957. https://doi.org/10.1016/j.ijbiomac.2023.127957 DOI: https://doi.org/10.1016/j.ijbiomac.2023.127957

Gawkowska, D., Cybulska, J., & Zdunek, A. (2018). Structure-related gelling of pectins and linking with other natural compounds: A review. Polymers, 10(7), 762. DOI: https://doi.org/10.3390/polym10070762

Gemechu, B., Keyata, E. O., Geleta, T. E., Gemede, H. F., & Bayata, A. (2024). Optimization of mango peel pectin extraction (Mangifera indica L.): For the production of jam and jelly. Applied Food Research, 4(1), 100411. https://doi.org/10.1016/j.afres.2024.100411 DOI: https://doi.org/10.1016/j.afres.2024.100411

Iñiguez-Moreno, M., Pizaña-Aranda, J. J. P., Ramírez-Gamboa, D., Ramírez-Herrera, C. A., Araújo, R. G., Flores-Contreras, E. A., Iqbal, H. M. N., Parra-Saldívar, R., & Melchor-Martínez, E. M. (2024). Enhancing pectin extraction from orange peel through citric acid-assisted optimization based on a dual response. International Journal of Biological Macromolecules, 263(Pt 1), 130230. https://doi.org/10.1016/j.ijbiomac.2024.130230 DOI: https://doi.org/10.1016/j.ijbiomac.2024.130230

Karim, R., Nahar, K., Zohora, F. T., Islam, M. M., Bhuiyan, R. H., Jahan, M. S., & Shaikh, M. A. A. (2022). Pectin from lemon and mango peel: Extraction, characterisation and application in biodegradable film. Carbohydrate Polymer Technologies and Applications, 4, 100258. https://doi.org/10.1016/j.carpta.2022.100258 DOI: https://doi.org/10.1016/j.carpta.2022.100258

Li, Y., Shuai, X., Zhang, M., Deng, X., Zhang, Y., Li, L., & Du, L. (2025). The physicochemical properties, structural characteristics, and rheological behavior of mango peel pectin with different degree of esterification. Journal of Future Foods, 7(1), 260–271. https://doi.org/10.1016/j.jfutfo.2024.12.013 DOI: https://doi.org/10.1016/j.jfutfo.2024.12.013

Mahmoud, M. H., & Azab, D. E.-S. H. (2025). Upcycling mango and pomegranate peel as pectin source: characterization, fat substitute and retarded lipid oxidation in caramel candy. Discover Food, 5(1), 37. https://doi.org/10.1007/s44187-025-00295-9 DOI: https://doi.org/10.1007/s44187-025-00295-9

Martínez-Hernández, A., Caamal-Cauich, I., Pat-Fernández, V. G., & Reza-Salgado, J. (2025). Indicadores de competitividad de las exportaciones de mango mexicano en el mercado mundial. Revista mexicana de ciencias agrícolas, 16(2), e3415. https://doi.org/10.29312/remexca.v16i2.3415 DOI: https://doi.org/10.29312/remexca.v16i2.3415

Martínez-Ramos, T., Benedito-Fort, J., Watson, N. J., Ruiz-López, I. I., Che-Galicia, G., & Corona-Jiménez, E. (2020). Effect of solvent composition and its interaction with ultrasonic energy on the ultrasound-assisted extraction of phenolic compounds from Mango peels (Mangifera indica L.). Food and Bioproducts Processing, 122, 41–54. https://doi.org/10.1016/j.fbp.2020.03.011 DOI: https://doi.org/10.1016/j.fbp.2020.03.011

Montgomery, D. C. (2017). Design and analysis of experiments. John Wiley & Sons.

Muslu Can, A., Metin Yildirim, R., & Karadag, A. (2024). The Properties of Pectin Extracted from the Residues of Vinegar-Fermented Apple and Apple Pomace. Fermentation, 10(11), 556. https://doi.org/10.3390/fermentation10110556 DOI: https://doi.org/10.3390/fermentation10110556

Öztürk, T., Özbek, H. N., & Koçak Yanık, D. (2024). Environmentally friendly approach to pectin extraction from grapefruit peel: Microwave-assisted high-pressure CO2/H2O. Foods, 13(3), 476. https://doi.org/10.3390/foods13030476 DOI: https://doi.org/10.3390/foods13030476

Pacheco-Jiménez, A. A., Basilio Heredia, J., Gutiérrez-Grijalva, E. P., Quintana-Obregón, E. A., & Muy-Rangel, M. D. (2022). Potencial industrial de la cáscara de mango (Mangifera indica L.) para la obtención de pectina en México. Tip revista especializada en ciencias químico-biológicas, 25. https://doi.org/10.22201/fesz.23958723e.2022.419 DOI: https://doi.org/10.22201/fesz.23958723e.2022.419

Pacheco-Jiménez, A. A., Lizardi-Mendoza, J., Heredia, J. B., Gutiérrez-Grijalva, E. P., Quintana-Obregón, E. A., & Muy-Rangel, M. D. (2024). Physicochemical characterization of pectin and mango peel (Mangifera indica L.) from Mexican cultivars. Heliyon, 10(15), e35184. https://doi.org/10.1016/j.heliyon.2024.e35184 DOI: https://doi.org/10.1016/j.heliyon.2024.e35184

Romdhane, M. B., Haddar, A., Ghazala, I., Jeddou, K. B., Helbert, C. B., & Ellouz-Chaabouni, S. (2017). Optimization of polysaccharides extraction from watermelon rinds: Structure, functional and biological activities. Food Chemistry, 216, 355–364. https://doi.org/10.1016/j.foodchem.2016.08.056 DOI: https://doi.org/10.1016/j.foodchem.2016.08.056

Rubio-Senent, F., Rodríguez-Gutiérrez, G., Lama-Muñoz, A., & Fernández-Bolaños, J. (2015). Pectin extracted from thermally treated olive oil by-products: Characterization, physico-chemical properties, in vitro bile acid and glucose binding. Food Hydrocolloids, 43, 311–321. https://doi.org/10.1016/j.foodhyd.2014.06.001 DOI: https://doi.org/10.1016/j.foodhyd.2014.06.001

Saelee, M., Myo, H., & Khat-Udomkiri, N. (2025). Sustainable pectin extraction from Riang husk using ultrasound-assisted extraction with deep eutectic solvents and its potential in antipollution products. Ultrasonics Sonochemistry, 114, 107256. https://doi.org/10.1016/j.ultsonch.2025.107256 DOI: https://doi.org/10.1016/j.ultsonch.2025.107256

Saravanan, R., & Jeevitha, G. C. (2024). Sustainable approach for utilization of mango peel wastes for pectin extraction by natural deep eutectic solvents. Journal of Food Processing and Preservation, 2024(1), 4540390. https://doi.org/10.1155/2024/4540390 DOI: https://doi.org/10.1155/2024/4540390

Sayed, M. A., Kumar, J., Rahman, M. R., Noor, F., & Alam, M. A. (2022). Effect of extraction parameters on the yield and quality of pectin from mango (Mangifera indica L.) peels. Discover Food, 2(1), 1–17. https://doi.org/10.1007/s44187-022-00029-1 DOI: https://doi.org/10.1007/s44187-022-00029-1

Şen, E., Göktürk, E., & Uğuzdoğan, E. (2024). Microwave-assisted extraction of pectin from onion and garlic waste under organic, inorganic and dual acid mixtures. Journal of Food Measurement and Characterization, 18(5), 3189–3198. https://doi.org/10.1007/s11694-024-02395-z DOI: https://doi.org/10.1007/s11694-024-02395-z

Shubhangi, S., Khalid Mehmood, W., Shaik Mahammad, M., Laksmi S, J., & Sneha Soundara, R. (2026). Review on pectin: Sources, properties, health benefits and its applications in food industry. Journal of Future Foods, 6(2), 205–219. https://doi.org/10.1016/j.jfutfo.2024.04.009 DOI: https://doi.org/10.1016/j.jfutfo.2024.04.009

Srikamwang, C., Willats, W. G. T., Bakshani, C. R., Sommano, S. R., & Wongkaew, M. (2024). Potentials of Mahachanok mango peel pectin in modulating glycaemic index in simulated in vitro carbohydrate digestion of meat product. Journal of Agriculture and Food Research, 18, 101304. https://doi.org/10.1016/j.jafr.2024.101304 DOI: https://doi.org/10.1016/j.jafr.2024.101304

Stubley, S. J., Cayre, O. J., Murray, B. S., & Torres, I. C. (2023). Emulsifying properties of sugar beet pectin microgels. Food Hydrocolloids, 137, 108291. https://doi.org/10.1016/j.foodhyd.2022.108291 DOI: https://doi.org/10.1016/j.foodhyd.2022.108291

Turan, O., Isci, A., Yılmaz, M. S., Tolun, A., & Sakiyan, O. (2024). Microwave-assisted extraction of pectin from orange peel using deep eutectic solvents. Sustainable Chemistry and Pharmacy, 37, 101352. https://doi.org/10.1016/j.scp.2023.101352 DOI: https://doi.org/10.1016/j.scp.2023.101352

Vellaisamy Singaram, A. J., & Ganesan, N. D. (2022). Modeling the influence of extraction parameters on the yield and chemical characteristics of microwave extracted mango (Mangifera indica L.) peel pectin by response surface methodology. Preparative Biochemistry & Biotechnology, 52(6), 711–723. https://doi.org/10.1080/10826068.2021.1989697 DOI: https://doi.org/10.1080/10826068.2021.1989697

Published

2026-08-01

How to Cite

Zárate Castillo, G., Damián Hernández, X., Chávez Portillo, M., Soto Reyes, N., Ruiz López, I. I., & TANIA. (2026). Valorization of Mango Peels for Pectin Production: Process Optimization and Physicochemical Evaluation. Revista Investigación Y Desarrollo En Ciencia Y Tecnología De Alimentos, 11(2), 65–75. https://doi.org/10.29105/idcyta.v11i2.167